Structure Elucidation by Modern NMR: A Workbook [Paperback]

During the last few years, routine applications of NMR techniques have been further developed. Spectrometers of the latest generation offer new types of experiments, such as spinlock and inverse-detected methods. In this third, revised and expanded edition, new methodology is introduced and incorporated into new exercises. In addition, a new chapter has been introduced which demonstrates the fully detailed interpretation of two typical examples.Introduction.- Methodology.- High Magnetic Fields. One-dimensional 1H,1H Correlation. Two-Dimensional 1H,13C One-Bond Correlation. Two-Dimensional 1H,13C Long-Range Correlation. NOE Experiments. 13C,13C-Correlation.- Two Demonstration Examples. Rearrangement of a Benzothiazepine to a Benzothiazole Derivative. Structure Elucidation of a Triterpene Saponin.- Exercises.- Strategies.- Solutions.A new spectrometer generation offers new types of experiments: new methodology will be introduced, incorporated in new exercises, two typical examples will be interpreted in full details. Includes supplementary material: sn.pub/extras