High-Resolution NMR Techniques in Organic Chemistry [Paperback]

High-Resolution NMR Techniques in Organic Chemistry, Third Edition describes the most important NMR spectroscopy techniques for the structure elucidation of organic molecules and the investigation of their behaviour in solution. Appropriate for advanced undergraduate and graduate students, research chemists and NMR facility managers, this thorough revision covers practical aspects of NMR techniques and instrumentation, data collection, and spectrum interpretation. It describes all major classes of one- and two-dimensional NMR experiments including homonuclear and heteronuclear correlations, the nuclear Overhauser effect, diffusion measurements, and techniques for studying protein-ligand interactions. A trusted authority on this critical expertise, High-Resolution NMR Techniques in Organic Chemistry, Third Edition is an essential resource for every chemist and NMR spectroscopist.

Preface 1 Introduction 2 Introducing High-Resolution NMR 3 Practical Aspects of High-Resolution NMR 4 One-Dimensional Techniques 5 Introducing Two-Dimensional and Pulsed Field Gradient NMR 6 Correlations Through the Chemical Bond I: Homonuclear Shift Correlation 7 Correlations Through the Chemical Bond II: Heteronuclear Shift Correlation 8 Separating Shifts and Couplings: J-Resolved and Pure Shift Spectroscopy 9 Correlations Through Space: The Nuclear Overhauser Effect 10 Diffusion NMR Spectroscopy 11 Protein-Ligand Screening by NMR 12 Experimental Methods 13 Structure Elucidation and Spectrum Assignment Appendix Subject Index

Timely and thorough, this revision describes the most important high-resolution NMR techniques used in elucidating the structure of organic molecules and examining their behavior in solution

High-Resolution NMR Techniques in Organic Chemistry, Third Edition describes the most important NMR spectroscopy techniques for the structure elƒ·