Organic Syntheses, Volume 94 [Hardcover]

The current volume continues the tradition of the Organic Syntheses series, providing carefully checked and edited experimental procedures that describe important synthetic methods, transformations, reagents, and synthetic building blocks or intermediates with demonstrated utility in organic synthesis. These significant and interesting procedures should prove worthwhile to many synthetic chemists working in increasingly diverse areas. A trusted guide for professionals in organic and medicinal chemistry in academia, government, and industries, including pharmaceuticals, fine chemicals, agrochemicals, and biotechnological products.

Preparation of Aryl Alkyl Ketenes 1
Nicholas D. Staudaher, Joseph Lovelace, Michael P. Johnson, and Janis Louie

Preparation of Diisopropylammonium Bis(catecholato)cyclohexylsilicate 16
Kingson Lin, Christopher B. Kelly, Matthieu Jouffroy, and Gary A.Molander

Continuous Flow Hydration of Pyrazine-2-carbonitrile in a Manganese Dioxide Column Reactor 34
Claudio Battilocchio, Shing-Hing Lau, Joel M. Hawkins, and Steven V. Ley

Site-Selective C-H Fluorination of Pyridines and Diazines with AgF₂ 46
Patrick S. Fier and John F. Hartwig

Site-Selective C-H Fluorination of Pyridines and Diazines with AgF2 46
Patrick S. Fier and John F. Hartwig

Ugi Multicomponent Reaction 54
André Boltjes, Haixia Liu, Haiping Liu, and Alexander Dömling

Palladium-catalyzed External-CO-Free Reductive Carbonylation of Bromoarenes 66
Hideyuki Konishi, Masataka FukudalÓ>