Structure Determination from Powder Diffraction Data [Hardcover]

The art of solving a structure from powder diffraction data has developed rapidly over the last ten years to the point where numerous crystal structures, both organic and inorganic, have been solved directly from powder data. However, it is still an art and, in contrast to its single crystal equivalent, is far from routine. The art lies not only in the correct application of a specific experimental technique or computer program, but also in the selection of the optimal path for the problem at hand. Written and edited by experts active in the field, and covering both the fundamental and applied aspects of structure solution from powder diffraction data, this book guides both novices and experienced practitioners alike through the maze of possibilities.

List of Contributors
1. Introduction,William I. F. David, Kenneth Shankland, Lynne B. McCusker and Christian Baerlocher
2. Structure determination from powder diffraction data: an overview,Anthony K. Cheetham
3. Laboratory X-ray powder diffraction,Daniel Lou?r
4. Synchrotron radiation powder diffraction,Peter W. Stephens, David E. Cox and Andrew N. Fitch
5. Neutron powder diffraction,Richard M. Ibberson and William I. F. David
6. Sample preparation, instrument selection and data collection,Roderick J. Hill and Ian C. Madsen
7. Autoindexing,Per-Erik Werner
8. Extracting integrated intensities from powder diffraction patterns,William I. F. David and Devinderjit S. Sivia
9. Experimental methods for estimating the relative intensities of overlapping reflections,Thomas Wessels, Christian Baerlocher, Lynne B. McCusker and William I. F. David
10. Direct methods in powder diffraction - basic concepts,Rene Peschar, Anke Etz, Jouk Jansen and Hendrick Schenk
11. Direct methods in powder diffraction - applications,Carmelo Giacovazzo, Angela Altomare, Maria Christina Burla, Benedetta Carrozzini, GiovlS2